A - Human Necessities – 61 – K
Patent
A - Human Necessities
61
K
A61K 9/14 (2006.01)
Patent
CA 2650395
The present invention provides a method of continuous precipitation and isolation of an amorphous solid particulate form of 3-[2-(3-tert-Butyl-ureido)-3,3-dimethyl-butyryl]-6,6-dimethyl-3-aza-bicyclo[3.1.0]hexane-2-carboxylic acid (2-carbamoyl-1-cyclobutylmethyl-2-oxo-ethyl)-amide having controlled physical properties. The present invention provides also pharmaceutical formulations comprising the precipitated compound.
La présente invention concerne une méthode de précipitation et d'isolement en continu d'une forme particulaire solide amorphe du (2-carbamoyl-1-cyclobutylméthyl-2-oxo-éthyl)-amide de l'acide 3-[2-(3-tert-butyl-uréido)-3,3-diméthyl-butyryl]-6,6-diméthyl-3-aza-bicyclo[3.1.0]hexane-2-carboxylique qui présente des propriétés physiques contrôlées. La présente invention concerne également des formules pharmaceutiques comprenant le composé précipité.
Cho Wing-Kee Philip
Liotta Vincenzo
Pridgen Christopher Stanley
Qiu Zhihui
Zarkadas Dimitrios
Ogilvy Renault Llp/s.e.n.c.r.l.,s.r.l.
Schering Corporation
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