Process for the preparation of...

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C - Chemistry, Metallurgy

07

D

260/308.3

C07D 285/08 (2006.01)

Patent

CA 1041102

ABSTRACT A process is provided for preparing 3-trichloromethyl- 5-chloro-1,2,4-thiadiazole in improved yields by reacting a defined molar excess trichloroacetamidine with trichloro- methanesulfenyl chloride while controlling pH of the reaction mixture. The present process may advantageously be employed in a batch or continuous process.

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