Process for the preparation of 2,2'-oxybis...

C - Chemistry – Metallurgy – 07 – C

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260/607.5

C07C 213/08 (2006.01) C07B 61/00 (2006.01) C07C 217/08 (2006.01) C07C 217/42 (2006.01)

Patent

CA 1336839

A process for the preparation of 2,2'-oxybis[N,N-dimethylethanamine] by reaction of 2,2'oxybisethanamine, hydrogen and formaldehyde having a reduced percentage of water on conventional fixed-bed hydrogenation catalysts. The reactants, especially the amine and formaldehyde, are heated to a predetermined temperature separate from each other, and then mixed with each other in the presence of the fixed-bed catalyst.

570783

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