Process for the preparation of...

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C - Chemistry, Metallurgy

07

C

C07C 19/12 (2006.01) C07C 17/10 (2006.01)

Patent

CA 2140443

A process for the preparation of 1,1,1-trichlorotrifluoroethane in which 1- chloro-2,2,2-trifluoroethane is subjected to chlor- ination by bringing the 1-chloro-2,2,2-trifluoroethane into contact with chlorine within a reaction vessel characterized in that the process is conducted in the liquid phase in the presence of a chemical free radical initiator under a pressure of from 1 to 20 bar and at a temperature within the range 50 to 120 °C, and the product is separated from the reaction mixture by fractional distilla- tion.

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