C - Chemistry – Metallurgy – 07 – C
Patent
C - Chemistry, Metallurgy
07
C
C07C 53/16 (2006.01) C07C 51/43 (2006.01) C07C 51/487 (2006.01)
Patent
CA 2192536
The present invention relates to a process for the preparation of a particularly pure monochloroacetic acid, in which, in a first step, a hydrogenation of a mixture of mono- and dichloroacetic acid is carried out to a residual content of dichloroacetic acid of 400 to 600 ppm and, in a second step, this mixture is subjected to melt crystallization. The hydrogenation is carried out with a heterogeneous catalyst which comprises 0.1 - 5.0% by weight of palladium and in which active charcoal or silicon dioxide is used as the support.
Ebmeyer Frank
Kampmann Detlef
Paulus-Von Russdorf Ulf Otto
Rossmeissl Rudolf
Clariant Gmbh
Fetherstonhaugh & Co.
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