Process for the preparation of aqueous solution of essential...

C - Chemistry – Metallurgy – 11 – B

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C11B 9/00 (2006.01) A01N 35/06 (2006.01) A01N 65/00 (2006.01) A23L 1/22 (2006.01) B01F 3/08 (2006.01) C11B 9/02 (2006.01) C11D 3/38 (2006.01) C11D 3/48 (2006.01) C11D 3/50 (2006.01) D06M 13/00 (2006.01) D06M 13/144 (2006.01)

Patent

CA 2270533

A process for the preparation of an aqueous hinokitiol solution, characterized by mixing hinokitiol or a hinokitiol-containing oil with water, boiling the obtained liquid mixture by heating, rapidly cooling the resulting liquid mixture, blowing oxygen into the liquid mixture under stirring, and storing the resulting mixture at 0.5 to 5 ~C. The process can give an aqueous solution of the water-insoluble essential oil having a concentration of up to about 40 %. This aqueous solution of the oil is easily handleable by virtue of its liquidness, and does not contain any organic solvent harmful to the human body, thus being highly safe. Further, the solution has antibacterial and/or microbicidal effect, thus being extremely useful as antibacterial agent, microbicide, and so on.

Cette invention concerne un procédé de préparation d'une solution aqueuse d'hinokitiol, qui consiste à mélanger de l'hinokitiol ou une huile contenant de l'hinokitiol avec de l'eau, à chauffer jusqu'à ébullition ledit mélange liquide, à refroidir rapidement le mélange liquide résultant, à injecter de l'oxygène dans le mélange liquide tout en remuant et à stocker le mélange résultant à une température comprise entre 0,5 et 5 ·C. Ce procédé permet d'obtenir une solution aqueuse de l'huile essentielle insoluble à une concentration pouvant atteindre 40 % environ. Ladite solution aqueuse de l'huile peut être facilement manipulée du fait qu'elle est à l'état liquide, et cette solution ne contient aucun solvant organique nocif pour le corps humain, ce qui en fait une solution extrêmement sure. Cette solution possède en outre des propriétés antibactériennes et/ou microbicides et s'avère donc particulièrement utile en tant qu'agent antimicrobien, microbicide, etc.

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