Process for the preparation of benzothiazolyl sulphenic acid...

C - Chemistry – Metallurgy – 07 – D

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260/246.6

C07D 413/12 (2006.01) C07D 277/80 (2006.01)

Patent

CA 1129860

PROCESS FOR THE PREPARATION OF BENZOTHIAZOLYL SULPHENIC ACID MORPHOLIDE Abstract of the Disclosure A process for the preparation of 2-benzothiazolyl sulphenic acid morpholide in an aqueous medium wherein the reaction product is separated in the molten state by heating the suspension with melting of the solid reaction product, subsequent rapid separation of the melt phase from the aqueous phase, and removal of volatile constituents still present in the melt phase, the sum of residence times amount- ing to not more than 15 minutes. Le A 18 561

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