Process for the preparation of diatomaceous filtration...

B - Operations – Transporting – 01 – J

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B01J 20/14 (2006.01) B01D 39/06 (2006.01)

Patent

CA 2135042

The invention relates to a process for obtaining diatomite filters with very low cristobalite concentration by means of bonding with silicate or silicic binders. The process of the invention comprises a step consisting of mixing a diatomite with an aqueous alkaline silicate or silicic acid solution, and a subsequent step consisting of calcination at a temperature not exceeding 850 degrees C. The invention also relates to a calcined diatomite filter having a cristobalite concentration of less than 1.5%, permeability of between 20 and 500 millidarcys, a cake density of less than 0.400 g/cm3 and < 15% oversize on a 50-micron sieve. This process can be used to obtain a diatomite filter having stable and adequate porosity.

Le procédé pour l'obtention d'agents filtrants diatomitiques à très faibles teneur en cristobalite par agglomération avec des liants silicatés ou siliciques faisant l'objet de l'invention comporte une étape de malaxage d'une diatomite avec une solution aqueuse d'un silicate alcalin ou d'acide silicique, et une étape ultérieure de calcination à une température n'excédant pas 850°C. L'invention a aussi pour objet un agent filtrant diatomitique calciné ayant une teneur en cristobalite inférieure à 1,5%, une perméabilité comprise entre 20 et 500 millidarcys, une densité gâteau inférieure à 0,400 g/cm3 et un refus au tamis de 50 µm inférieur à 15%. Le procédé selon l'invention présente l'avantage de permettre l'obtention d'un agent filtrant diatomitique ayant une porosité stable et suffisante.

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