Process for the preparation of glycerol dichlorohydrins

Details Process for the preparation of glycerol dichlorohydrins Process for the preparation of glycerol dichlorohydrins

C - Chemistry, Metallurgy

07

C

260/636.9

C07C 31/34 (2006.01)

Patent

CA 1105491

ABSTRACT OF THE DISCLOSURE Process for the preparation of glycerol dichloro- hydrins by reacting allyl chloride and chlorine in an aqueous medium. An aqueous emulsion of allyl chloride in a water/allyl chloride weight ratio of at least 25:1 is continuously delivered to a tubular reactor, together with gaseous chlorine in a molar quantity not exceeding that of allyl chloride fed in, and reacted therein with said chlorine under adiabatic conditions, maintaining an inlet temperature of 10-50°C, a residence time of at least 15 seconds and a linear velocity of the reagent mixture of at least 0.5 m/sec.

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