Process for the preparation of n,n-diisopropyl-2-...

Details Process for the preparation of n,n-diisopropyl-2-... Process for the preparation of n,n-diisopropyl-2-...

C - Chemistry, Metallurgy

07

D

260/309.3

C07D 277/80 (2006.01)

Patent

CA 1269986

Abstract of the Disclosure PROCESS FOR THE PREPARATION OF N,N-DIISOPROPYL-2-BENZOTHIAZYL-SULFENAMIDE There is disclosed a process for the preparation of N,N-diisopropylbenzothiazyl-2-sulfenamide which comprises contacting an aqueous mixture of diisopropylamine and 2-mercaptobenzothiazole with an oxidizing agent in the presence of sufficient acid to neutralize the excess base, if any, in the oxidizing agent wherein the molar ratio of diisopropylamine to 2-mercaptobenzothiazole is at least 1.5 to 1.

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