Process for the preparation of n,n'-tetrathiodimorpholine

Details Process for the preparation of n,n'-tetrathiodimorpholine Process for the preparation of n,n'-tetrathiodimorpholine

C - Chemistry, Metallurgy

07

D

260/245.5

C07D 295/26 (2006.01)

Patent

CA 1299177

Abstract of the Disclosure IMPROVED PROCESS FOR THE PREPARATION OF N,N'-TETRATHIODIMORPHOLINE There is disclosed a process for the preparation of N,N'-tetrathiodimorpholine wherein an admixture of morpholine and elemental sulfur is oxidized with air or oxygen in the presence of iron salts or iron complexes in combination with zinc compounds such as ZnCl2 and ZnO to yield N,N'-tetrathiodimorpholine.

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