C - Chemistry – Metallurgy – 07 – C
Patent
C - Chemistry, Metallurgy
07
C
260/618
C07C 39/10 (2006.01) C07C 37/055 (2006.01) C07C 41/34 (2006.01) C07C 43/225 (2006.01)
Patent
CA 1154461
ABSTRACT OF THE DISCLOSURE A process for the preparation of phloroglucinol is disclosed. The process comprises reacting hexachloro- benzene with sodium propylate or sodium isopropylate, in a molar ratio of from about 1:3 to about 1:20, in an aprotic solvent, at a temperature from about 50 to about 250°C, to form trichlorophloroglucinol tripropylether, or trichloro- phloroglucinol triisopropylether. The latter compounds are dechlorinated to form phloroglucinol tripropylether or phloroglucinol triisopropylether, with the use of metallic sodium, and subsequently hydrolyzed to form phloroglucinol.
335801
Maegerlein Helmut
Zielke Rainer
Akzona Incorporated
Swabey Ogilvy Renault
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