Process for the preparation of random copolymers

Details Process for the preparation of random copolymers Process for the preparation of random copolymers

C - Chemistry, Metallurgy

08

F

402/645

C08F 210/16 (2006.01) C08F 2/34 (2006.01) C08F 4/64 (2006.01) C08F 210/06 (2006.01)

Patent

CA 1312173

- 21 - PROCESS FOR THE PREPARATION OF RANDOM COPOLYMERS Abstract of the Invention A process for the copolymerization of at least the two comonomers, propylene and ethylene, comprising contacting the comonomers in the gas phase in at least one reaction zone, under polymerization conditions, with a catalyst system comprising (i) a catalyst precursor, which includes magnesium, titanium, halogen, and as an inner electron donor, a mono- or polycarboxylic acid ester; (ii) a hydrocarbylaluminum cocatalyst; and (iii) as a selectivity control agent, a mono- or polycarboxylic acid ester, provided that the selectivity control agent is different from the inner electron donor, wherein the atomic ratio of aluminum to titanium is in the range of about 5 to about 300, with the proviso that the temperature in the reaction zone is in the range of about 50°C to about 110°C; the molar ratio of aluminum to selectivity control agent is in the range of about 0.5 to about 5; the propylene partial pressure is in the range of about 50 to about 450 psi; and the ethylene partial pressure is in the range of about 0.25 to about 25 psi. D-15868

599393

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