Process for the production of alkaline earth metal alkyl...

C - Chemistry – Metallurgy – 07 – C

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253/97, 260/615.

C07C 39/235 (2006.01) C10M 129/10 (2006.01) C10M 135/30 (2006.01) C10M 159/22 (2006.01)

Patent

CA 1246615

ABSTRACT OF THE DISCLOSURE Alkaline earth metal alkyl phenates are produced by reacting at elevated temperature, in the presence or absence of sulphur, an alkyl phenol with an alkaline earth metal base in the presence as solvent of either an alkylene or polyalkylene alkyl ether of formula R(OR1)xOR2 wherein R is C1 to C6 alkyl, R1 is alkylene, R2 is hydrogen or C1 to C6 alkyl and x is an integer in the range 1 to 6 and as catalyst an inorganic halide, preferably a hydrogen halide, an ammonium halide, an alkaline earth metal halide, a zinc halide or an aluminium halide. It is preferred to add an acid. Furthermore, carbon dioxide is preferably incorporated in the phenate.

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