Process for the production of n-formyl-.alpha.-l-aspartyl-l-...

C - Chemistry – Metallurgy – 07 – K

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530/5.06

C07K 5/06 (2006.01) C07K 1/02 (2006.01) C07K 5/075 (2006.01)

Patent

CA 1302648

ABSTRACT OF THE DISCLOSURE There is disclosed a process for producing N-formyl-?-L-aspartyl-phenylalanine methyl ester. The process comprises reacting N-formyl-L-aspartic acid anhydride and L-phenylalanine methyl ester in a reaction solvent and in the presence of acetic acid or a mixture of acetic acid and formic acid in a complete mixing type continuous reaction mode. This process has the advantage that it is possible to greatly increase the ratio between N-formyl-?-L-aspartyl-L- phenylalanine methyl ester and its isomer, the N-formyl-.beta.-L- -aspartyl-L-phenylalanine methyl ester, in the reaction product.

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