Process for the purification of 5h-dibenz(b,f)azepine

Details Process for the purification of 5h-dibenz(b,f)azepine Process for the purification of 5h-dibenz(b,f)azepine

C - Chemistry, Metallurgy

07

D

C07D 223/22 (2006.01)

Patent

CA 2165894

Process for the purification of 5H-dibenz[b,f]a- zepine, which comprises evaporating 5H-dibenz[b,f]azepine under reduced pressure from a reaction mixture obtained by catalytic dehydrogenation of 10,11-dihydro-5H-dibenz- [b,f]azepine in the 1st step and depositing it as a solid, suspending the deposited product in an aromatic hydrocarbon in the 2nd step and then isolating pure 5H- dibenz[b,f]azepine.

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