Process for the solvent-free manufacture of compound...

C - Chemistry – Metallurgy – 06 – B

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C06B 31/06 (2006.01) C06B 21/00 (2006.01) C06B 25/34 (2006.01) C06B 29/08 (2006.01) C06B 31/40 (2006.01) C06B 45/10 (2006.01)

Patent

CA 1256702

Abstract The present invention relates to the field of compound pyrotechnic products. The invention relates to a three-step, solvent-free process for the manufacture of compound pyrotechnic products containing a thermosetting binder obtained by reaction of a polyhydroxylated prepolymer with a di- isocyanate, which process is characterized in that: - in a first step the said prepolymer is mixed with an energetic charge and with a quantity of diisocyanate representing 50 to 90% of the required stoichiometric quantity, - in a second step the remainder required to attain the said stoichiometric quantity is added and, after mixing, the pasty mixture thus obtained is extruded, - in a third step the crosslinking of the thermoset- ting binder is completed hot. The invention makes it possible to obtain industrially, by extrusion, small-diameter pyrotechnic products con- taining a thermosetting binder without restriction on the "pot life" period. The invention is particularly suitable for the production of compound propellent powders for arms.

502564

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