Processes for producing monoammonium adipate from...

C - Chemistry – Metallurgy – 07 – C

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C07C 51/43 (2006.01) C12P 7/44 (2006.01) C12P 13/00 (2006.01) C07C 55/14 (2006.01)

Patent

CA 2738166

A process for making MAA from a clarified DAA-containing fermentation broth includes (a) distilling the broth to form an overhead that includes water and ammonia, and a liquid bottoms that includes MAA, at least some DAA, and at least about 20 wt% water; (b) cooling the bottoms to a temperature sufficient to cause the bottoms to separate into a DAA-containing liquid portion in contact with a MAA-containing solid portion that is substantially free of DAA; (c) separating the solid portion from the liquid portion; and (d) recovering the solid portion.

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