Production method of an insect pheromone

C - Chemistry – Metallurgy – 07 – D

Patent

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260/353.8

C07D 493/18 (2006.01) C07C 29/143 (2006.01) C07C 33/05 (2006.01) C07C 43/315 (2006.01) C07C 45/65 (2006.01) C07C 45/72 (2006.01) C07C 45/76 (2006.01) C07C 49/687 (2006.01) C07D 309/12 (2006.01) C07D 311/94 (2006.01) C07D 407/12 (2006.01) C07D 493/08 (2006.01) C07F 7/18 (2006.01)

Patent

CA 1224794

ABSTRACT OF THE DISCLOSURE A process for producing 3,3,7-trimethyl-2,9- dioxatricyclo[3.3.1.04,7]nonane useful as an insect pheromone and having the formula, Image which comprises reducing 1,5,5-trimethyl-7-endo-tert- butyldimethylsilyloxy-4-oxabicyclo[4.2.0]octan-3-one with diisobutylaluminum hydride, and treating with an acid, after desilylation.

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