Production of aqueous solutions of cationic thermosetting...

C - Chemistry – Metallurgy – 08 – L

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117/196, 400/782

C08L 77/10 (2006.01) D21H 3/58 (1980.01)

Patent

CA 1149983

ABSTRACT OF THE DISCLOSURE A durable aqueous solution of a thermosetting resin having a relatively high solid content which imparts a high degree of wet strength to paper, is pro- duced by the reaction of an aliphatic dicarboxylic acid with a polyalkylenepolyamine to form a polyamidopoly- amine, which is successively subjected to reaction with epichlorohyrin, the first reaction being carried out using a molar ration of aliphatic dicarboxylic acid to polyalkylenepolyamine of 1 : 1.0 to 1.2 and continued until the viscosity ar 25°C of 50% aqueous solution of resulting polyamidopolyamine reaches 400 to 1,000 cps, and the second reaction being carried out using epichloro- hydrin in an amount of 1.6 to 1.7 moles per mole of the polyamide secondary amine and continued until the viscosity at 25°C of 15% aqueous solution of the resulting product reaches 30 to 150 cps.

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