Production of butanediol

C - Chemistry – Metallurgy – 07 – C

Patent

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Details

C07C 29/141 (2006.01) C07C 27/04 (2006.01) C07C 29/38 (2006.01) C07C 31/20 (2006.01)

Patent

CA 2591448

The catalytic hdrogenation of HBA and/or HMPA is improved by either or both of (1) increasing the temperature in the hydrogenation zone from about 50 to 70~C at the inlet to above 80~C at the outlet and (2) raising the pH of the hydrogenation feed to 4.5 - 6.0 before hydrogenation.

L'hydrogénation catalytique de HBA et/ou HMPA est améliorée par (1) l'augmentation de la température dans la zone d'hydrogénation entre environ 50 et 70 °C à l'entrée pour atteindre plus de 80 °C à la sortie et/ou (2) l'élévation du pH de la charge d'hydrogénation à 4,5 6,0 avant hydrogénation.

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