Production of mannitol and higher mannosaccharide alcohols

C - Chemistry – Metallurgy – 07 – C

Patent

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204/53, 260/632.

C07C 29/14 (2006.01) C07C 29/141 (2006.01) C07C 31/26 (2006.01) C25B 3/04 (2006.01)

Patent

CA 1229350

ABSTRACT A method for hydrolyzing coffee extraction residue materials to produce manno-saccharides having a degree of polymerization from 1 to 10 and subsequently neutralizing and reducing said mixture of manno-saccharides to their corresponding alcohols. The coffee material, preferably spent coffee gounds from a commercial percolation system, is hydrolyzed in a Plug Flow tubular reactor in the presence of an acid catalyst, such as sulfuric acid. Depending on the time, temperature, pressure and catalyst concen- tration selected, manno-saccharide or mannose is produced. The manno-saccharides or mannose produced are separated from coffee residue material in the form of a syrup and neutralized with calcium hydroxide. The neutralized mixture of manno-saccharides or mannose is reduced to their corresponding alcohols or mannitol

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