Production of methyldichlorophosphane

Details Production of methyldichlorophosphane Production of methyldichlorophosphane

C - Chemistry, Metallurgy

07

F

260/537.6

C07F 9/28 (2006.01) C07F 9/52 (2006.01)

Patent

CA 1087206

PRODUCTION OF METHYLDICHLOROPHOSPHANE ABSTRACT OF THE DISCLOSURE: Production of methyldichlorophosphane. The compound is made by reacting methane and phos- phorus trichloride in a reaction zone in which a temperature higher than 500°C is maintained. More specifically, hot reaction gas coming from the reaction zone is mechanically freed from solid matter, and the reaction gas freed from solid matter is passed to a quenching zone in which it is quenched with liquefied reaction mixture having 0.3 to 5 weight% of an organic barium compound or a non-ionic surfactant dis- solved therein.

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