Purification of tertiary hydroperoxides containing primary...

Details Purification of tertiary hydroperoxides containing primary... Purification of tertiary hydroperoxides containing primary...

C - Chemistry, Metallurgy

07

C

260/649.5

C07C 407/00 (2006.01) C07C 409/04 (2006.01)

Patent

CA 2001037

ABSTRACT Primary and secondary hydroperoxide contaminants in a tertiary hydroperoxide composition obtained by oxidation of a branched hydrocarbon are removed by contacting the tertiary hydroperoxide with a carboxylic acid derivative such as an anhy- dride and a basic compound such as sodium hydroxide. The inven- tion provides a method for purifying a tertiary hydroperoxide such as tertiary butyl hydroperoxide with minimal loss of the desired tertiary hydroperoxide.

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