Purification process for photographic image-forming...

C - Chemistry – Metallurgy – 09 – B

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260/178

C09B 29/00 (2006.01)

Patent

CA 1117523

PURIFICATION PROCESS FOR PHOTOGRAPHIC IMAGE-FORMING SULFONAMIDO COMPOUNDS ABSTRACT OF THE DISCLOSURE A process for purifying a photographic image- forming sulfonamido compound comprises the steps of: a. preparing a first solution by dissolving an unpurified image-forming sulfonamido compound in an aprotic solvent; b. removing impurities from said first solution by, at least once: i. mixing said first solution with an immiscible nonpolar, low-boiling organic solvent to form a mixture of said first solution and a second solution comprising said immiscible nonpolar, low-boiling organic solvent and at least a portion of said impurities, and ii. separating said first solution from said second solution; and c. recovering purified image-forming sulfonamido compound from said first solution. The process is useful in the purification of a nondiffusible sulfonamdio compound which is alkali-cleavable upon oxidation to release a diffusible sulfonamido color-providing moiety.

322808

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