Real-time imaging and spectroscopy during microwave assisted...

B - Operations – Transporting – 01 – J

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B01J 19/12 (2006.01)

Patent

CA 2617424

An instrument and associated method are disclosed for conducting microwave assisted chemical reactions. The instrument includes a microwave cavity, preferably a closed microwave cavity, for conducting microwave assisted chemical reactions, and a source for applying microwave radiation within the cavity and to a vessel and its contents. The instrument also includes an illumination source for illuminating the vessel and its contents, as well as means for visually observing the vessel and its contents, an infrared detector for monitoring the temperature of the vessel and its contents, and means for preventing the illumination source from saturating the infrared detector, thereby enabling concurrent visual observation and infrared monitoring.

La présente invention concerne un instrument et le procédé associé pour réaliser des réactions chimiques assistées par micro-ondes. L~instrument comprend une cavité micro-ondes, de préférence une cavité micro-ondes fermée, pour réaliser des réactions chimiques assistées par micro-ondes, et une source servant à appliquer une radiation micro-ondes à l~intérieur de la cavité et à un récipient et son contenu. L~instrument comprend également une source d'éclairage permettant d~éclairer le récipient et son contenu, ainsi que des moyens d'observation visuelle du récipient et de son contenu et un détecteur infrarouge servant à contrôler la température du récipient et de son contenu, et des moyens pour empêcher la saturation par la source d~éclairage du détecteur infrarouge, ce qui permet une observation visuelle et un contrôle infrarouge simultanés.

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