Recovery of ammoniacal copper with organogels

B - Operations – Transporting – 01 – J

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149/14, 403/2, 5

B01J 39/20 (2006.01) B01J 45/00 (2006.01) C01G 3/00 (2006.01) C22C 3/00 (2006.01) C23F 1/46 (2006.01)

Patent

CA 1269491

RECOVERY OF AMMONIACAL COPPER WITH NOVEL ORGANOGELS ABSTRACT There is disclosed novel copper ion-exchange media and processes for the recovery of cupric ion from ammoniacal copper solutions and for the recovery of spent printed circuit board etchant. The novel ion- exchange media comprise hydrophobic nonporous polymer plasticized and swollen with a monomeric organic liquid copper ion-exchange agent such as beta-diketones or hydroxyoximes. A novel copper ion-complexing agent, 1-n-octylphenyl-p-1,3-butanedione, is also disclosed. The processes essentially comprise contacting the ammoniacal cupric ion-containing solution or spent etchant with the novel copper ion-exchange media to extract copper in cupric ion form. Copper can be recovered therefrom by conventional methods such as acid stripping and electrowinning.

471530

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