Removing hydrocarbon impurities from acetic acid production...

C - Chemistry – Metallurgy – 07 – C

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C07C 51/12 (2006.01) C07C 51/48 (2006.01) C07C 53/08 (2006.01)

Patent

CA 2756813

A method for removing hydrocarbon impurities from an acetic acid production intermediate is disclosed. The method comprises extracting the intermediate with a hydrocarbon extracting agent. The extraction is preferably performed with the alkane distillation bottom stream which comprises methyl iodide, acetic acid, and hydrocarbon impurities. The extraction forms a light phase which comprises the hydrocarbon impurity and the extracting agent and a heavy phase which comprises methyl iodide and acetic acid. The extraction heavy phase is optionally recycled to the alkane distillation or to the carbonylation reaction.

La présente invention concerne un procédé destiné à éliminer des impuretés hydrocarbures d'un intermédiaire permettant la production d'acide acétique. Le procédé comprend l'étape consistant à extraire l'intermédiaire à l'aide d'un agent d'extraction des hydrocarbures. L'extraction est, de préférence, effectuée alors que le courant de la queue de distillation des alcanes comprend de l'iodure de méthyle, de l'acide acétique, et des impuretés hydrocarbures. L'extraction permet d'obtenir une phase légère comprenant les impuretés hydrocarbures et l'agent d'extraction et une phase lourde comprenant l'iodure de méthyle et l'acide acétique. La phase lourde provenant de l'extraction est éventuellement réutilisée dans la distillation des alcanes ou dans la réaction de carbonylation.

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