Secondary c10-c18 surfactant alcohols

C - Chemistry – Metallurgy – 07 – C

Patent

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Details

C07C 31/125 (2006.01) C07C 29/17 (2006.01) C07C 43/11 (2006.01) C07C 45/50 (2006.01) C07C 45/62 (2006.01) C07C 45/73 (2006.01) C07C 45/74 (2006.01) C07C 305/06 (2006.01) C07C 305/10 (2006.01) C07F 9/09 (2006.01) C07F 9/11 (2006.01) C11D 1/14 (2006.01) C11D 1/29 (2006.01) C11D 1/34 (2006.01) C11D 1/72 (2006.01)

Patent

CA 2415715

The invention relates to secondary C10 to C18 surfactant alcohols of the general formula (I), wherein R represents methyl or ethyl and R' represents a linear or branched alkyl group with 6-13 C atoms, excepting 5-ethyl-2-nonanol and 6-ethyl-3-decanol, in addition to fatty alcohol alkoxylates, alkyl phosphates, alkyl sulphates, alkyl ether phosphates and alkyl ether sulphates. The secondary C10 to C18 surfactant alcohols can be produced by a simple aldol condensation of linear or branched saturated or unsaturated C7-C14 aldehydes, excepting 2-ethyl hexanal, with acetone or methyl ethyl ketone and the subsequent hydrogenation of the condensation product. In the preferred method, the aldol condensation is heterogenically catalysed under hydrogenation conditions and the saturated ketone that has been formed is subsequently hydrogenated.

Alcools tensioactifs secondaires C¿10? à C¿18? de formule générale (I) dans laquelle R représente méthyle ou éthyle et R' représente un reste alkyle linéaire ou ramifié ayant 6 à 13 atomes de C, à l'exception du 5-éthyle-2-nonanol et du 6-éthyle-3-décanol, ainsi que les alcoxylates d'alcools gras, les phosphates d'alkyle, les sulfates d'alkyle, les phosphates d'alkyléther et les sulfates d'alkyléther pouvant être obtenus à partir desdits alcools tensioactifs. Lesdits alcools tensioactifs C¿10? à C¿18? secondaires peuvent être préparés par simple condensation aldolique entre des aldéhydes C¿7? à C¿14? linéaires ou ramifiés, saturés ou insaturés, à l'exception du 2-éthylhexanal, et une acétone ou la méthyléthylcétone, puis par hydrogénation du produit de condensation. Le procédé préféré est un procédé selon lequel la condensation aldolique est catalysée de manière hétérogène dans des conditions d'hydrogénation, et la cétone saturée formée est ensuite hydrogénée.

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