Semi-continuous photochemical method and device therefor

Details Semi-continuous photochemical method and device therefor Semi-continuous photochemical method and device therefor

B - Operations, Transporting

01

J

B01J 19/12 (2006.01) B01J 19/24 (2006.01) C07C 319/04 (2006.01) C07C 319/18 (2006.01) C07C 321/14 (2006.01)

Patent

CA 2444021

The invention concerns a method for semi-continous photochemical synthesis which consists in using a reactor comprising two zones (1, 3), the radiating part (2a) of the lamp(s) being totally immersed in a first zone (1) which is completely filled with a reaction medium and overflows through an overflow unit into the second zone (3) whereof the volume is sufficient to contain the volume of the reaction medium derived from the first zone (1) and substantially corresponding to the volume of the reagent(s) gradually introduced.

Dans le procédé de synthèse photochimique en mode semi-continu selon l'invention, on utilise un réacteur comprenant deux zones (1, 3), la partie rayonnante (2a) de la ou des lampe(s) (2) étant totalement immergée dans une première zone (1) qui est complètement remplie de milieu réactionnel et se déverse par trop-plein dans une seconde zone (3) dont le volume est suffisant pour contenir le volume de milieu réactionnel provenant de la première zone (1) et correspondant sensiblement au volume du ou des réactif(s) introduit(s) progressivement.

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