Silica polymorph and process for preparaing same

C - Chemistry – Metallurgy – 01 – B

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C01B 33/12 (2006.01) B01D 53/02 (2006.01) B01J 20/10 (2006.01) C01B 37/02 (2006.01)

Patent

CA 1093278

10638 SILICA POLYMORPH AND PROCESS FOR PREPARING SAME ABSTRACT OF DISCLOSURE Large crystals of a silica polymorph having a characteristic x-ray diffraction pattern, a specific gravity of 1.70 ? 0.05 g/cc.and a mean refractive index of 1.39 ? 0.01 after calcination in air at 600°C., are prepared by a hydrothermal process in which fluoride anions are included in the reaction mixture. The crystals, which can be as large as 200 microns, exhibit a substantial absence of infrared adsorption in the hydroxyl-stretching region and also exhibit an exceptional degree of hydrophobicity. S P E C I F I C A T I O N _ _ _ _ _ _ _ _ _ _ _ _ _

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