Single-compartment electrolytic hydrodimerization process

Details Single-compartment electrolytic hydrodimerization process Single-compartment electrolytic hydrodimerization process

C - Chemistry, Metallurgy

25

B

204/53.5

C25B 3/10 (2006.01) C07C 69/34 (2006.01)

Patent

CA 1039230

SINGLE-COMPARTMENT ELECTROLYTIC HYDRODIMERIZATION PROCESS ABSTRACT OF THE DISCLOSURE In a process for hydrodimerizing an olefinic nitrile, amide or ester by electrolyzing an aqueous solution of the olefinic compound, quaternary ammonium cations and an alkali metal phos- phate, borate or carbonate in a single-compartment cell, anode corrosion problems are substantially avoided by use of a cell having an anode consisting essentially of carbon steel. Even at high temperatures and current densities, the corrosion rate of such an anode is surprisingly low. Even lower rates of corrosion of such an anode are achieved when the electrolyzed solution contains an alkali metal phosphate and an alkali metal borate. -1-

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