Solid supports for peptide synthesis

Details Solid supports for peptide synthesis Solid supports for peptide synthesis

C - Chemistry, Metallurgy

08

F

402/340, 402/453

C08F 212/08 (2006.01) B01J 19/08 (2006.01) C07K 1/04 (2006.01) C08F 212/36 (2006.01)

Patent

CA 1312991

BG-D-10 SOLID SUPPORTS FOR PEPTIDE SYNTHESIS Abstract of the Disclosure Solid supports of the formula P-C6H4-CH(R1)-NHCOCH2Q-C6H4-COCH(R2)-X wherein P and the 1,4-phenylene (C6H4) to which it is attached is a copoly(styrene-divinylbenzene) matrix, Q is oxo or thio, R1 is methyl, phenyl, 4-methylphenyl or 4-methoxyphenyl, R2 is hydro- gen, lower alkyl, phenylalkylene or phenyl and X is chloro, bromo or iodo are disclosed. They can be prepared by coupling an amine-containing copoly- (styrene-divinylbenzene) resin, for example, benz- hydrylamine resin, with a 4-(.alpha.-haloalkanoyl)phenoxy- acetic acid or a 4-(.alpha.-haloalkanoyl)phenylthioacetic acid. The solid supports are useful for solid phase peptide synthesis.

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