Synthesis of...

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C - Chemistry, Metallurgy

07

C

C07C 225/12 (2006.01) C07C 213/00 (2006.01) C07C 213/02 (2006.01) C07C 217/74 (2006.01) C07F 15/02 (2006.01)

Patent

CA 2462108

Compositions comprising (.plusmn.)-2-((dimethylamino)methyl)cyclohexanone, a transition-metal salt, and an organic solvent and methods ofpreparing (.plusmn.)-cis-2-((dimethylamino)methyl)-l-(aryl)cyclohexanols, in particular (.plusmn.)-cis-2-((dimethylamino)methyl)-1-(3-methoxyphenyl)cyclohexanol, are disclosed herein. In one embodiment, the (.plusmn.)-2- ((dimethylamino)methyl)cyclohexanone and transition-metal salt are in the form of a (.plusmn.)-2-((dimethylamino)methyl)cyclohexanone:transition-metal salt complex. In another embodimemt, aryl is 3-methoxyphenyl.

L'invention concerne des compositions comprenant de la (.plusmn.)-2-((diméthylamino)méthyl)cyclohexanone, un sel de métal de transition, et un solvant organique, ainsi que des procédés de préparation de (.plusmn.)-cis-2-((diméthylamino)méthyl)-l-(aryl)cyclohexanols, en particulier de (.plusmn.)-cis-2-((diméthylamino)méthyl)-1-(3-méthoxyphényl)cyclohexanol. Dans un mode de réalisation, la (.plusmn.)-2-((diméthylamino)méthyl)cyclohexanone et le sel de métal de transition sont sous la forme de complexe (.plusmn.)-2-((diméthylamino)méthyl)cyclohexanone:sel de métal de transition. Dans un autre mode de réalisation, le groupe aryle est un groupe 3-méthoxyphényle.

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