Synthesis of 2-amino-2-deoxyglycoses and 2-amino-2-...

Details Synthesis of 2-amino-2-deoxyglycoses and 2-amino-2-... Synthesis of 2-amino-2-deoxyglycoses and 2-amino-2-...

C - Chemistry, Metallurgy

07

H

260/227

C07H 5/04 (2006.01)

Patent

CA 1111417

"SYNTHESIS OF 2-AMINO-2-DEOXYGLYCOSES AND 2-AMINO-2-DEOXYGLYCOSIDES FROM GLYCALS" ABSTRACT OF THE DISCLOSURE 0-acylated-2-azido-2-deoxy glycosyl nitrates are used to prepare 0-acylated-2-azido-2-deoxy glycosyl halides. The halides are useful in the preparation of 0-acetylated-2-azido-2-deoxy glycosides, which in turn can be reduced to 2-amino-2-deoxy glycosides. Of particular interest are the syntheses of 2-amino-2-deoxy glycosides which correspond to the terminal units of the antigenic determinant for the human A blood group. Attachment of these glycosides to a solid support provides immunoabsorbents which effectively and preferentially absorb anti-A-antibodies from blood plasma.

367510

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