Synthesis of bis(dichloroalumino)-methane

Details Synthesis of bis(dichloroalumino)-methane Synthesis of bis(dichloroalumino)-methane

C - Chemistry, Metallurgy

07

F

260/432.3

C07F 5/06 (2006.01)

Patent

CA 1294627

SYNTHESIS OF BIS(DICHLOROALUMINO)METHANE ABSTRACT OF THE DISCLOSURE A process for the synthesis of bis(dichloroalumino)- methane, with a lessened danger of runaway reaction, entails the gradual addition of methylene bromide to a heated mixture of aluminum and methylene chloride. An aluminum alkyl activator is also advantageously present as a scavenger for moisture and oxygen to prevent undesired oligomer formation. The bis(dichloroalumino)methane produced by the process of the present invention can be used as a reagent in various types of chemical syntheses.

580949

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