Synthesis of deoxybiotinyl hexamethylenediamine-dota

Details Synthesis of deoxybiotinyl hexamethylenediamine-dota Synthesis of deoxybiotinyl hexamethylenediamine-dota

C - Chemistry, Metallurgy

07

D

C07D 495/04 (2006.01)

Patent

CA 2607262

A process for the synthesis of deoxybiotinyl hexamethylenediamine-DOTA is herein described. Said process comprises reacting biotinyl hexamethylenediamine with tri-t-butyl-DOTA in the presence of benzotriazol-1- yl-oxytripyrrolidinophosphonium hexafluorophosphate, as the condensing agent, and triethylamine, as the base.

L'invention concerne un procédé de synthèse du désoxybiotinyle hexaméthylènediamine-DOTA. Ledit procédé comprend la réaction de l'hexaméthylènediamine de biotinyle avec du tri-t-butyle-DOTA en présence de benzotriazol-1-yl-oxytripyrrolidinophosphonium hexafluorophosphate, servant d'agent condensateur, et de triéthylamine, servant de base.

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