Synthesis of ethers of n-propanoldiamines

Details Synthesis of ethers of n-propanoldiamines Synthesis of ethers of n-propanoldiamines

C - Chemistry, Metallurgy

07

D

260/325.5

C07D 207/04 (2006.01) C07D 295/088 (2006.01) C07D 295/13 (2006.01)

Patent

CA 1192907

-8- SYNTHESIS OF ETHERS OF N-PROPANOLDIAMINES ABSTRACT OF THE DISCLOSURE A process for preparing .beta.-[(2-methylpropoxy) methyl]-N-phenyl-N-(phenylmethyl)-l-pyrrolidineethanamine hydrochloride hydrate in which isobutanol is reacted with epichlorohydrin, the product is reacted with thionyl chloride, and the compound thus obtained condensed with n-benzylaniline. In accordance with the invention, the condensing step is carried out using sodium hydride as the condensing agent.

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