Synthesis of fluoromethyl ether

Details Synthesis of fluoromethyl ether Synthesis of fluoromethyl ether

C - Chemistry, Metallurgy

07

C

C07C 43/12 (2006.01) C07C 41/01 (2006.01) C07C 41/16 (2006.01)

Patent

CA 2111762

ABSTRACT A novel process for synthesizing difluoromethyl methyl ether for use as regrigerants and blowing agents, etc. is hereby disclosed. This process involves (1) feeding chlorodifluoromethane at a rate from about 0.5 to 5 grams of feed gas per gram of solution per minute through a sodium methoxide in methanol or basic ion exchange slurry in methanol; (2) removing the gaseous product and the unreacted chlorodifluoromethane continuously; and (3) separating difluoromethyl ether from the unreacted chlorodifluoromethane.

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