Synthesis of heterocyclic amines via the reaction of...

Details Synthesis of heterocyclic amines via the reaction of... Synthesis of heterocyclic amines via the reaction of...

C - Chemistry, Metallurgy

07

D

260/247.9

C07D 265/30 (2006.01) C07D 295/02 (2006.01) C07D 295/023 (2006.01)

Patent

CA 1151646

ABSTRACT This invention relates to an improved process fox producing morpholine and its derivates by reacting ammonia and dialkylene glycol. The improvement resides in continuously charging the dialkylene glycol and ammonia to a trickle bed reactor, operating the reactor under conditions such that the dialkylene glycol is maintained as a discontinuous liquid phase and the morpholine formed is predominantly in the vapor phase.

372539

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