Synthesis of tetradecahydroundecaborate (-1) from...

Details Synthesis of tetradecahydroundecaborate (-1) from... Synthesis of tetradecahydroundecaborate (-1) from...

C - Chemistry, Metallurgy

01

B

23/3, 260/590.6

C01B 35/00 (2006.01) C07F 5/02 (2006.01)

Patent

CA 1113679

ABSTRACT OF THE INVENTION The tetradecahydroundecaborate(-1) anion is synthesized from a metal borohydride by heating a suspension of the borohydride ion in a solvent, such as diglyme, with agitation at a temperature of from 85°C. to about 135°C. and adding an alkyl halide. The B11B14-anion obtained is useful in the synthesis of decaborane, an intermediate in formation a carborane-based polymers.

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