Thiophene purification

C - Chemistry – Metallurgy – 07 – D

Patent

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Details

C07D 333/10 (2006.01) C07B 63/00 (2006.01)

Patent

CA 2261195

Pour purifier un thiophène contenant des mercaptans, on oxyde ces derniers en polysulfures et sépare le thiophène par distillation. L'oxydation des mercaptans par le soufre est de préférence effectué à l'aide d'un catalyseur basique. La réaction est rapide et pratiquement complète, et permet de former des polysulfures lourds aisément séparables par distillation du thiophène.

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