Two phase process for the preparation of azole and azoline...

Details Two phase process for the preparation of azole and azoline... Two phase process for the preparation of azole and azoline...

C - Chemistry, Metallurgy

07

D

260/311.1, 260/3

C07D 235/28 (2006.01) C07D 277/78 (2006.01) C07D 285/04 (2006.01) C07D 285/08 (2006.01) C07D 285/125 (2006.01) C10M 135/32 (2006.01) C10M 135/36 (2006.01)

Patent

CA 1069906

ABSTRACT OF THE DISCLOSURE Azole and azoline disulfides useful as corrosion inhibitors and antiwear agents are prepared by the halogen-induced coupling of a thiol reactant e.g., hydrocarbyl mercaptans, with a metal azole thiolate, e.g. the potassium salt of 3,5-bis-mercapto 1,2,4-thiadiazole or 2,5-bis-mercapto 1,3,4 thiadiazole in a 2-phase reaction medium comprising a mixture of a hydrocarbon and water.

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