Volatile fluorinated beta-ketoimines and associated metal...

Details Volatile fluorinated beta-ketoimines and associated metal... Volatile fluorinated beta-ketoimines and associated metal...

C - Chemistry, Metallurgy

07

C

260/428, 260/579

C07C 251/08 (2006.01) C07F 1/08 (2006.01) C07F 7/18 (2006.01) C07F 15/06 (2006.01) C23C 16/18 (2006.01)

Patent

CA 1330803

ABSTRACT Fluorinated .beta.-ketoimine ligands and highly volatile .beta.-ketoiminato metal complexes of the ligands are synthesized by silylating a fluorinated .beta.-diketone to form a silylenolether, and subsequently reacting the silylenolether with a primary amine to form the desired ligand having the structural formula: Image wherein R1 and R2 are independently linear or branched perfluorinated, C1-C8 alkyl groups and R3 is any organic functionality such as a C1-C8 alkyl, phenyl or hydroxyalkyl group, all of which can be partially or fully fluorinated. The corresponding metal complex is formed by treating the ligand with 3 metal halide.

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