Production of o,o-dialkyl-s-(benzazimidomethyl)-thiol...

Details Production of o,o-dialkyl-s-(benzazimidomethyl)-thiol... Production of o,o-dialkyl-s-(benzazimidomethyl)-thiol...

C - Chemistry, Metallurgy

07

F

260/248.6

C07F 9/6521 (2006.01)

Patent

CA 1126273

Abstract Chemagro 227 PRODUCTION OF O,O-DIALKYL-S-(BENZAZIMIDOMETHYL)- THIOL PHOSPHORIC ACID ESTERS ABSTRACT OF THE DISCLOSURE In the reaction of a halomethylbenzazamide with an O,O-di-lower alkyl-thiolphosphoric acid ester to form an ester in accordance with the equation Image Image in which Y is oxygen or sulfur, and M is an alkali metal or ammonium cation, the improvement which comprises starting the reaction at a pH from about 2.5 to 5.5, whereby the desired reaction product is produced in higher yield and assay. Chemagro 227

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