C - Chemistry – Metallurgy – 07 – F
Patent
C - Chemistry, Metallurgy
07
F
260/537.6
C07F 9/28 (2006.01) C07F 9/34 (2006.01) C07F 9/52 (2006.01)
Patent
CA 1204450
PROCESS FOR MAKING CHLOROPHOSPHANES, PHOSPHINIC ACID CHLORIDES OR THIOPHOSPHINIC ACID CHLORIDES, AND NOVEL ISO- MERIC MIXTURE CONSISTING OF CHLORO-PHOSPHABICYCLONONANES ABSTRACT OF THE DISCLOSURE The disclosure relates to a process for making chloro- phosphanes from primary or secondary phosphanes, or phosphi- nic acid chlorides or thiophosphinic acid chlorides from se- condary phosphane oxides or sulfides, wherein the respective starting materials are reacted with hexachloroethane at tem- peratures of 20 to 180°C. The disclosure also provides as a novel chemical substance an isomeric mixture consisting of 9-C1-9-phosphabicyclononane [3.3.1] and 9-C1-9-phosphabi- cyclononane [4.2.1].
434906
Clariant Gmbh
Fetherstonhaugh & Co.
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