Process for washing and obtaining solids of slurry

C - Chemistry – Metallurgy – 07 – C

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260/623.7

C07C 37/84 (2006.01) C07C 39/16 (2006.01)

Patent

CA 1291170

27979-6 ABSTRACT OF THE DISCLOSURE A process for washing and obtaining solids of a slurry comprises feeding a slurry containing the adduct of bisphenol A with phenol crystallized from a phenol solution of bisphenol A to a first solid-liquid separator to separate solids from the slurry, transferring the solids separated by the first solid-liquid separator to an agitation tank in which the solids are reslurried, feeding the slurry obtained in the agitation tank to a second solid-liquid separator, said second solid-liquid separator being intended to obtain the solids from the slurry discharged from the agitation tank, and permitting the admission of a washing solvent to wash the solids, and permitting the filtrate and washings to be recovered independently, feeding the washing solvent to the second solid-liquid separator, feeding all of the washings from the second solid-liquid separator to the agitation tank, feeding a part of the filtrate from the second solid-liguid separator to the agitation tank, and discharging the remainder of the filtrate from the system. The process makes it possible to produce a high-purity adduct of bisphenol A with phenol and hence high-purity bisphenol A.

591416

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