Method of preparation of dithiocarbamate complexes of...

Details Method of preparation of dithiocarbamate complexes of... Method of preparation of dithiocarbamate complexes of...

C - Chemistry, Metallurgy

07

F

260/383, 260/427

C07F 11/00 (2006.01)

Patent

CA 1264473

ABSTRACT METHOD OF PREPARATION OF DITHIOCARBAMATE COMPLEXES OF MOLYBDENUM (VI) An improved process for preparing dihydrocarbyl substituted dithiocarbamates of molybdenum (VI) wherein an alkali metal ammonium or substituted ammonium salt of a dihydrocarbyl substituted dithio- carbamate is recited with an alkali metal molydate in the presence of an organic acid. The process is carried out in an inert atmosphere and within a relatively narrow range of temperatures. The dihydrocarbyl substituted dithiocarbamate of molydenum (VI) may be recrystallized after preparation to increase its purity. The dihydrocarbyl sub- stituted dithiocarbamate of molybdenum (VI) is produced at a temper- ature within the range from about -10°C to about +25°C at a pH during neutralization within the range from about 5.0 to about 8Ø

536617

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