Synthesis of 1-acetoxy-2-methylnaphthalene

Details Synthesis of 1-acetoxy-2-methylnaphthalene Synthesis of 1-acetoxy-2-methylnaphthalene

C - Chemistry, Metallurgy

07

C

C07C 69/14 (2006.01) C07C 67/297 (2006.01) C07C 69/035 (2006.01)

Patent

CA 2212906

A one pot process is provided in which a Mannich base of the formula 5 is reacted with acetic anhydride to produce a diacetate derivative. Without any intermediate isolation, the derivative is hydrogenated to produce a reaction mixture containing 1-acetoxy-2-methylnaphthalene which is readily precipitated from the reaction mixture by addition of water.

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