Synthesis of organic phosphines

Details Synthesis of organic phosphines Synthesis of organic phosphines

C - Chemistry, Metallurgy

07

F

C07F 9/6568 (2006.01) C07F 9/50 (2006.01) C07F 9/6558 (2006.01)

Patent

CA 2291503

9-phosphabicyclononanes are prepared by adding phosphine to a 1,5-cyclooctadiene in the presence of a free radical initiator in a polar solvent. Use of a polar solvent favours the formation of [3.3.1]- and [4.2.1]-9- phosphabicyclononanes over other secondary or tertiary phosphine products.

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